Services

Metallographic Sample Preparation

Metallographic specimen preparation, also called precision metallurgical sample preparation, is a key step in performing reliable metallurgical testing. This type of testing often involves evaluating the microstructure of materials through optical magnification or scanning electron microscopy (SEM). It is essential that all microscopy sample preparation, including SEM preparation, be completed carefully and properly for image clarity.

How Does LTI Conduct Metallographic Sample Preparation?

The preparation of a sample is crucial to the accuracy of the metallographic analysis. Microstructure and hardness of a sample must be revealed, and you must be confident that what you see is actually there, not just something created during preparation. You can’t skip steps during metallographic sample preparation.

LTI Metallographic Sample Preparation Capabilities

  • Extent of decarburization and carburization
  • Grain size
  • Intergranular attack
  • Depth of alpha case in titanium alloys
  • Percent spheroidization
  • Inclusion rating
  • Volume fraction of various phases or second phase particles in metals
  • Evaluation of welds
  • Evaluation and identification of typical microstructures of metals to confirm structure or property relationships (e.g., tempered martensite in steels)
  • Precision cutting
  • 1.5″ and 2″ standard mounts
  • Nonstandard mounting
  • Thermoset and thermoplastic mounting
  • Cold mounting
  • Automatic grinding and polishing
  • Immersion, swab, and electrolytic etching

Samples are prepared in our metallurgical lab using precision cutting, mounting, grinding, and polishing techniques, as well as etching when required.

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